Methyl 3-(benzyloxy)-1-((tert-butoxycarbonyl)amino)-4-oxo-1,4-dihydropyridine-2-carboxylate
Methyl 3-(benzyloxy)-1-((tert-butoxycarbonyl)amino)-4-oxo-1,4-dihydropyridine-2-carboxylate
Factory Supply industrial standard Methyl 3-(benzyloxy)-1-((tert-butoxycarbonyl)amino)-4-oxo-1,4-dihydropyridine-2-carboxylate 2136287-59-5 In Stock
- Molecular Formula:C19H22N2O6
- Molecular Weight:374.393
- Density:1.27±0.1 g/cm3(Predicted)
2136287-59-5 Relevant articles
Pyridone-containing polycyclic derivative inhibitor as well as preparation method and application thereof
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Paragraph 0163; 0166-0169, (2021/05/12)
The invention relates to a pyridone-cont...
PYRIDOPYRAZINE AND PYRIDOTRIAZINE INHIBITORS OF INFLUENZA VIRUS REPLICATION
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, (2020/05/06)
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, (2020/11/09)
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, (2020/12/29)
The invention discloses a spiro pyridone...
2136287-59-5 Process route
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870-46-2
t-butoxycarbonylhydrazine
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3-benzyloxy-4-oxo-4H-pyran-2-carboxylic acid methyl ester
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2136287-59-5
methyl 1-((tert-butoxycarbonyl)amino)-3-(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxylic acid
| Conditions | Yield |
|---|---|
|
With
pyridinium p-toluenesulfonate;
In
N,N-dimethyl acetamide;
at 60 ℃;
for 20.5h;
|
82% |
|
With
pyridinium p-toluenesulfonate;
In
N,N-dimethyl acetamide;
at 60 ℃;
for 15h;
|
80% |
|
With
pyridinium p-toluenesulfonate;
In
N,N-dimethyl acetamide; N,N-dimethyl-formamide;
at 60 ℃;
|
78% |
|
With
pyridinium p-toluenesulfonate;
In
N,N-dimethyl acetamide;
at 60 ℃;
for 12h;
|
73% |
|
3-benzyloxy-4-oxo-4H-pyran-2-carboxylic acid methyl ester;
With
pyridinium p-toluenesulfonate;
In
N,N-dimethyl acetamide;
at 65 - 70 ℃;
for 7h;
t-butoxycarbonylhydrazine;
In
N,N-dimethyl acetamide;
at 65 - 70 ℃;
Temperature;
|
65% |
|
With
toluene-4-sulfonic acid;
In
N,N-dimethyl acetamide;
at 55 ℃;
|
44% |
|
With
pyridinium p-toluenesulfonate;
In
N,N-dimethyl acetamide;
at 60 ℃;
for 9h;
|
122.7 g |
|
With
pyridinium p-toluenesulfonate;
In
N,N-dimethyl acetamide;
at 60 ℃;
for 16h;
|
-
-
870-46-2
t-butoxycarbonylhydrazine
-
-
119736-16-2
3-(benzyloxy)-1-((tert-butoxycarbonyl)amino)-4-oxo-1,4-dihydropyridine-2-carboxylic acid ethyl ester
-
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77-78-1
dimethyl sulfate
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-
2136287-59-5
methyl 1-((tert-butoxycarbonyl)amino)-3-(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxylic acid
| Conditions | Yield |
|---|---|
|
3-(benzyloxy)-1-((tert-butoxycarbonyl)amino)-4-oxo-1,4-dihydropyridine-2-carboxylic acid ethyl ester; dimethyl sulfate;
With
sodium hydrogencarbonate;
In
N,N-dimethyl acetamide;
at 25 ℃;
for 7h;
t-butoxycarbonylhydrazine;
With
pyridinium p-toluenesulfonate;
In
N,N-dimethyl acetamide;
at 60 ℃;
for 3h;
|
77% |
2136287-59-5 Upstream products
-
119736-16-2
3-(benzyloxy)-1-((tert-butoxycarbonyl)amino)-4-oxo-1,4-dihydropyridine-2-carboxylic acid ethyl ester
-
870-46-2
t-butoxycarbonylhydrazine
-
118-71-8
Maltol
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61049-69-2
3-O-benzylmaltol
2136287-59-5 Downstream products
-
1985605-59-1
(R)-12-((S)-7,8-difluoro-6,11-dihydrodibenzo[b,e]thiepin-11-yl)-7-hydroxy-3,4,12,12a-tetrahydro-1H-[1,4]oxazino[3,4-c]pyrido[2,1-f][1,2,4]triazine-6,8-dione
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1985607-70-2
7-(benzyloxy)-3,4,12,12a-tetrahydro-1H-[1,4]oxazino[3,4-c]pyrido [2,1-f][1,2,4]triazine-6,8-diketone
